利用微反应器设计了连续合成二甲基二烯丙基氯化铵的新工艺，考察了反应温度、物料摩尔比、停留时间对反应的影响，并通过单因素条件对实验工艺进行优化。结果表明，较优的实验条件为：n（二甲胺）∶n（氢氧化钠）∶n（氯丙烯）=1∶1∶2.1、反应温度为45℃、停留时间为11 min，此时产品收率为92%。与传统间歇"一步法"工艺相比，该微反应工艺简化了操作，缩短了反应时间，并且提高了收率。

A novel continuous synthesis process for dimethyldiallylammonium chloride in a microreactor is designed.The influences of reaction temperature,molar ratio of raw materials and residence time on the reaction are observed,and the process is modified from single-factor conditional experiment.It is found that the product yield reaches 92% under the optimized conditions that n(dimethylamine)∶n(sodium hydroxide)∶n(allyl chloride)=1∶1∶2.1,reaction temperature is 45℃ and residence time is 11 min.Compared with traditional one-step process,the microreactor process can simplify procedures,shorten reaction time,and realize higher yield.