将一维纳米纤维素纤维（NCFs）作为MoS₂的有效分散剂，通过超临界二氧化碳干燥和高温碳化过程制备碳纳米球纤维（CNPFs）/MoS₂纳米杂化气凝胶电极材料。利用SEM、EDS、FT-IR和电化学测试等手段对杂化电极材料的组成、结构和电化学性能进行表征。结果表明，一定量的NCFs是MoS₂的稳定分散剂，可以有效阻碍MoS₂纳米片层的团聚。所制备的CNPFs/MoS₂杂化气凝胶电极材料在0.5 A/g电流密度下的质量比电容高达366.84 F/g，而且具有优异的循环稳定性。

Carbon nanosphere fibers (CNPFs)/MoS₂ nanohybrid aerogel electrode materials are prepared by supercritical carbon dioxide drying-high temperature carbonization process,using one-dimensional nanocellulose fibers (NCFs) as an effective dispersant for MoS₂.The composition,structure and electrochemical performance of the hybrid electrode materials are characterized via SEM,EDS,FT-IR and electrochemical measurements.It is shown that a certain amount of NCFs is a stable dispersant for MoS₂,which can effectively prevent MoS₂ nanosheets from agglomeration.Mass specific capacitance of the prepared CNPFs/MoS₂ hybrid aerogel electrode material reaches as high as 366.84 F·g^-1 at a current density of 0.5 A·g^-1.In addition,it has excellent cycle stability.