硅钼蓝-紫外可见分光光度法测定里松温泉水中硅的含量

陈秋娟, 谢微, 韦师

现代化工 ›› 2017, Vol. 37 ›› Issue (12) : 210 -214.

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现代化工 ›› 2017, Vol. 37 ›› Issue (12) : 210-214. DOI: 10.16606/j.cnki.issn0253-4320.2017.12.051
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硅钼蓝-紫外可见分光光度法测定里松温泉水中硅的含量

    陈秋娟, 谢微, 韦师
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Determination of silicon content in Lisong hot spring water by silicon molybdenum blue UV-visible spectrophotometry

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摘要

采用硅钼蓝-紫外可见分光光度法测定里松温泉源头水中硅的质量浓度。实验结果表明:体系中硅钼蓝的λmax=814 nm,硅质量浓度在0~0.019 63 μg/mL范围内与吸光度具有良好的线性关系,其线性方程为y=0.212 5+1.197 2x,相关系数为0.999 6,回收率为96.47%~105.0%,RSD为0.358%~1.191%。该方法操作简便、精密度好、准确率高,可用于温泉水中硅质量浓度的测定。

Abstract

The content of silicon in the source water of Lisong hot spring is detected by silicon molybdenum blue UV-visible spectrophotometry method.It is indicated by experimental results that λmax of silicon molybdenum blue in the system is 814 nm and the mass concentration of silicon within the scope of 0-0.019 63 μg·mL-1 has good linear relationship with absorbance.The linear equation is y=0.212 5+1.197 2x and the correlation coefficient is 0.999 6.The recovery rate is in the range of 96.47%-105.0% and the RSD is in the range of 0.358%-1.191%.This method is easy to operate and has high precision and accuracy,which can be used for the determination of silicon content in hot spring water.

关键词

硅钼蓝 / / 里松温泉水 / 紫外可见分光光度法

Key words

silicon molybdenum blue / silicon / Lisong hot spring water / UV-visible spectrophotometry

Author summay

陈秋娟(1983-),女,硕士研究生,讲师,研究方向为天然产物提取、纯化与分析,2002090099@163.com

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硅钼蓝-紫外可见分光光度法测定里松温泉水中硅的含量[J]. 现代化工, 2017, 37(12): 210-214 DOI:10.16606/j.cnki.issn0253-4320.2017.12.051

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