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现代化工  2021, Vol. 41 Issue (4): 234-237    DOI: 10.16606/j.cnki.issn0253-4320.2021.04.049
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金纳米星的制备及对塑化剂的快速检测
赖宇明
北京科技大学国家材料服役安全科学中心, 北京 100083
Preparation of gold nanostars and its application in fast detection of plasticizers
LAI Yu-ming
National Center for Materials Service Safety, University of Science and Technology Beijing, Beijing 100083, China
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摘要 采用两步法合成了金纳米星,通过消光光谱和透射电镜的表征,发现金纳米星的表面有多个针尖状纳米结构。针尖状结构末端的尺寸5~10 nm,可形成多个拉曼热点。将其作为表面增强拉曼散射(SERS)活性基底,通过拉曼光谱检测了塑化剂DBP的含量,检出限可达到10 ng。金纳米星可作为一种灵敏的SERS活性基底为食品、生活用品等环境中的塑化剂提供快速的检测。
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赖宇明
关键词:  塑化剂  DBP  表面增强拉曼散射  SERS  金纳米星    
Abstract: Gold nanostars,which have many needle-like nano structures,are synthesized by two-step method and characterized by extinction spectrum and transmission electron microscope.The end of needle like nano structure has a size of 5-10 nm,which can form many Raman hot spots.Gold nanostars are used as the active substrate of surface-enhanced Raman scattering to detect the content of plasticizer dibutyl phthalate (DBP),the detection limit achieves 10 ng.Gold nanostars have a potential application in providing rapid detection of plasticizers in food,daily necessities and other environments.
Key words:  plasticizer    DBP    surface-enhanced Raman scattering    SERS    gold nanostars
收稿日期:  2020-06-29      修回日期:  2021-03-05          
ZTFLH:  R155  
基金资助: 高校国家重大基础设施开放共享和运行维护经费(FRF-GF-18-003A)
通讯作者:  赖宇明(1987-),女,博士,工程师,研究方向为金属表面及金属溶液界面的分子性质,通讯联系人,yuminglai@ustb.edu.cn。    E-mail:  yuminglai@ustb.edu.cn
引用本文:    
赖宇明. 金纳米星的制备及对塑化剂的快速检测[J]. 现代化工, 2021, 41(4): 234-237.
LAI Yu-ming. Preparation of gold nanostars and its application in fast detection of plasticizers. Modern Chemical Industry, 2021, 41(4): 234-237.
链接本文:  
https://www.xdhg.com.cn/CN/10.16606/j.cnki.issn0253-4320.2021.04.049  或          https://www.xdhg.com.cn/CN/Y2021/V41/I4/234
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