减压逆流多效精馏回收膜工业废水中的DMAC

王洪海, 韦晓晓, 薛璐璐, 王钊, 周琦, 李春利

现代化工 ›› 2019, Vol. 39 ›› Issue (8) : 226 -230,234.

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现代化工 ›› 2019, Vol. 39 ›› Issue (8) : 226-230,234. DOI: 10.16606/j.cnki.issn0253-4320.2019.08.048
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减压逆流多效精馏回收膜工业废水中的DMAC

    王洪海, 韦晓晓, 薛璐璐, 王钊, 周琦, 李春利
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Technical research on recovery of DMAC from wastewater by vacuum countercurrent multi-effect distillation

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摘要

针对膜工业中所产生的质量分数为5%~15%的N,N-二甲基乙酰胺(DMAC)废水,提出了分离DMAC废水减压逆流的双效、三效和四效精馏工艺流程。通过实验和Aspen流程模拟对多效精馏的工艺进行了研究。利用响应面法(RSM)对多效流程进行了优化,以最小年度总费用(TAC)为目标函数,确定了回收废水中DMAC最佳方案为减压逆流三效精馏工艺。

Abstract

Aiming at treating N,N-dimethylacetamide (DMAC) wastewater with a content of 5%-15% produced in the membrane industry,the double-effect,three-effect and four-effect distillation processes for vacuum countercurrent of DMAC wastewater system are proposed.These multi-effect distillation processes are studied through experiments and Aspen process simulation.Response surface method (RSM) is used to optimize these multi-effect processes.With the minimum total annual cost (TAC) as the objective function,the vacuum countercurrent three-effect distillation process is determined as the best solution for recovering DMAC from wastewater.

关键词

N,N-二甲基乙酰胺 / TAC / 响应面法 / 废水处理 / 多效精馏

Key words

N,N-dimethylacetamide / TAC / response surface method / wastewater treatment / multi-effect distillation

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减压逆流多效精馏回收膜工业废水中的DMAC[J]. 现代化工, 2019, 39(8): 226-230,234 DOI:10.16606/j.cnki.issn0253-4320.2019.08.048

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