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摘要
采用炭吸附沉淀法制备铁酸铋(BiFeO3)纳米粉体,通过TG-DTA、XRD、UV-Vis、TEM等仪器分析其结构和性能。在1 000 W镝灯的照射下,以降解甲基橙(MO)为探针反应考察其光催化性能。结果显示,活性炭在铁酸铋粉体制备过程中有效抑制了团聚和烧结现象。煅烧温度为500℃下制备的铁酸铋粉体的晶化程度高、颗粒分布均匀、粒径小,在120 min内对甲基橙的降解率可达91.2%。
Abstract
BiFeO3 nano powders are prepared through carbon adsorption co-precipitation method, and their structure and properties are characterized by means of thermogravimetric analyzer, X-ray diffractometer, UV-Vis spectrophotometer and transmission electron microscope.The photocatalytic properties of BiFeO3 nano powders are also evaluated with the degradation of methyl orange as the probe reaction under the irradiation of a 1, 000 W dysprosium lamp.It is shown that activated carbon has effectively suppressed the agglomeration and sintering phenomena during the preparation of BiFeO3 powder.BiFeO3 powder calcined at 500℃ shows high crystallinity, uniform particle distribution and small particle size, over which the degradation rate of methyl orange can reach 91.2% within 120 min.
关键词
铁酸铋
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甲基橙
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光催化性能
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共沉淀法
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炭吸附法
Key words
FeBiO3
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methyl orange
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photocatalytic properties
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co-precipitation
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carbon adsorption
Author summay
黄强(1996-),男,硕士生,研究方向为光催化降解有机污染物,150247248738@163.com
炭吸附纳米铁酸铋粉体的制备及其光催化性能研究[J].
现代化工, 2021, 41(S1): 126-128,133 DOI:10.16606/j.cnki.issn0253-4320.2021.S.025