以Bi （NO₃）₃·5H₂O和KBr为原料，采用一步溶剂热法制备一系列不同石墨烯质量分数的BiOBr/Graphene复合物。利用XRD、SEM、BET和UV-Vis对合成的BiOBr/Graphene进行表征，结果表明合成产品为三维花球状的BiOBr/Graphene。以罗丹明B （RhB）为光催化降解底物、负载石墨烯质量分数为0.75%、合成温度为160℃、合成时间为12 h、乙二醇（EG）和N，N-二甲基甲酰胺（DMF）为溶剂时，30 min最大降解率达到96.36%。

A series of 3D flower-like BiOBr/graphene composites with different graphene contents are synthesized via a simple one-step solvothermal method with Bi(NO₃)₃·5H₂O and KBr as raw materials.Through characterization by XRD,SEM,BET and UV-Vis,the as-synthesized product is verified to be 3D flower-like microspheres consisting of BiOBr/graphene.The maximum degradation rate of Rhodamine B can reach 96.36% in 30 min when the BiOBr/graphene composite that is synthesized with 0.75% of graphene160℃ for 12 h is used as photocatalyst,and a mixture between ethylene glycol and N,N dimethylformamide is used as solvent.

伍水生(1982-),男,博士,副教授,研究方向为纳米光催化材料,wuss2005@126.com