固体润滑材料高纯二硫化钼生产工艺改进

成兰兴, 谷中鸣, 师传兴, 邵国斌, 丁为公, 张碧波

现代化工 ›› 2017, Vol. 37 ›› Issue (10) : 156 -158.

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现代化工 ›› 2017, Vol. 37 ›› Issue (10) : 156-158. DOI: 10.16606/j.cnki.issn0253-4320.2017.10.037
工艺与设备

固体润滑材料高纯二硫化钼生产工艺改进

    成兰兴, 谷中鸣, 师传兴, 邵国斌, 丁为公, 张碧波
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Improvement of production process for high purity molybdenum disulfide solid lubricant material

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摘要

通过对原有生产工艺进行改进,加入除铁专用的助溶剂,变原有多段除铁为一段除铁,使生产过程周期由原工艺的24 h缩短为15 h,生产效率提高50%,酸性废水减少60%。加入除铁专用的助溶剂,使铁的去除率由原工艺的78.0%提高到93.3%。通过生产连续运行考察,在最佳操作条件下,产品中铁质量分数降低到0.08%,收率由原工艺的88%提高到93%,经济效益显著。

Abstract

The original production process is improved with the addition of specific co-solvent for removing iron and one stage removal of iron replacing multi stage removal of iron for a period in addition to iron.After improvement,the production cycle is shortened to 15 hours from the original 24 hours,the production efficiency increases by 50%,and emission amount of acidic wastewater reduces by 60%.With the addition of specific co-solvent,the removal rate of iron increases from 78.0% to 93.3%.Through continuous operation,the iron content in the product drops to 0.08% under the optimum operating conditions,and the yield increases from 88% in original process to 93%.The economic benefit is remarkable.

关键词

二硫化钼 / 一段除铁 / 工艺改进

Key words

molybdenum disulfide / one stage removal of iron / process improvement

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固体润滑材料高纯二硫化钼生产工艺改进[J]. 现代化工, 2017, 37(10): 156-158 DOI:10.16606/j.cnki.issn0253-4320.2017.10.037

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